@unpublished {2406, title = {Mining multimodal fatigue data using reasoning foundation models and formalized domain knowledge}, year = {2025}, abstract = {

The scarcity and expense of fatigue data limits optimal design of components and constrains companies to a few well qualified materials when safety-critical applications are concerned. This research investigates different strategies to improve extraction of structured information from unstructured scientific literature\–-to date the largest corpus of fatigue information. Successful generative extraction is within reach considering latest foundation vision and reasoning language model (VLM/RLM) developments. In this work, a schema-based extraction is attempted for which an object-oriented fatigue data schema is designed. The schema provides labels, definitions and type-constraints for the target entities as contextual domain knowledge to the VLM/RLM model. The importance of nuanced target field definitions within the schema and constrained decoding is explored. Furthermore, the schema-based approach is gradually extended to form two agentic language model systems, one which utilizes a step-wise, human-inspired approach to first determine discriminative cues from fatigue S-N diagrams and one further applying dynamic knowledge augmentation. The latter dynamic workflow exploits the synergy of reasoning language models and ontologies by performing logical reasoning and web-search for dynamic knowledge augmentation and hallucination detection. On this rather complex fatigue data extraction task, requiring hierarchical pattern recognition and multimodal extraction, an overall F1-score of 0.82 is achieved, while fields contained in the narrative text modality are extracted with an F1-score of 0.92. The strengths and weaknesses of all models and methodologies are thoroughly discussed and extensions to our workflows are proposed.

}, author = {Mohanty, Jyoti Prakash and Thomas, Akhil and Pollock, Tresa M and Durmaz, Ali Riza} } @article {2411, title = {Modeling the evolution of slip localization: Realization of link to material strength}, journal = {Acta Mater.}, volume = {299}, year = {2025}, pages = {121314}, author = {Ahmadikia, Behnam and Bean, Chris and Stinville, Jean-Charles and Pollock, Tresa M and Beyerlein, Irene J} } @article {2361, title = {Machine learning based damage identification in SiC/SiC composites from acoustic emissions using autoencoders}, journal = {Compos. B Eng.}, volume = {287}, year = {2024}, pages = {111802}, author = {Muir, C and Gibson, T and Hilmas, A and Almansour, A S and Sevener, K and Kiser, J D and Pollock, T M and Daly, S and Smith, C} } @article {2291, title = {Materials design for hypersonics}, journal = {Nat. Commun.}, volume = {15}, year = {2024}, pages = {3328}, abstract = {

Hypersonic vehicles must withstand extreme conditions during flights that exceed five times the speed of sound. These systems have the potential to facilitate rapid access to space, bolster defense capabilities, and create a new paradigm for transcontinental earth-to-earth travel. However, extreme aerothermal environments create significant challenges for vehicle materials and structures. This work addresses the critical need to develop resilient refractory alloys, composites, and ceramics. We will highlight key design principles for critical vehicle areas such as primary structures, thermal protection, and propulsion systems; the role of theory and computation; and strategies for advancing laboratory-scale materials to manufacturable flight-ready components.

}, author = {Peters, Adam B and Zhang, Dajie and Chen, Samuel and Ott, Catherine and Oses, Corey and Curtarolo, Stefano and McCue, Ian and Pollock, Tresa M and Eswarappa Prameela, Suhas} } @article {2256, title = {Misfit and the mechanism of high temperature and low stress creep of Ni-base single crystal superalloys}, journal = {Acta Materialia}, volume = {264}, year = {2024}, pages = {119576}, abstract = {

The present work proposes a new elementary deformation mechanism which governs high temperature and low stress creep of single crystal superalloys (SXs), where the misfit between the \γ- and the \γ\′-phase plays a central role. In the coherent two phase SX microstructure, there is a tendency to minimize the overall elastic strain energy. This is accomplished by the formation of dislocation networks in the \γ-phase close to the \γ/\γ\’-interfaces. The stress fields of the network dislocations and misfit stresses accommodate each other to keep the overall strain energy of the system at a minimum. Previous work has shown that dynamic recovery is associated with knitting-out reactions, where dislocations from the network shear the \γ\’-phase and annihilate with dislocations of opposite sign on the other side of the \γ\’-phase region. Due to the presence of the misfit this results in an increase of elastic strain energy which is counteracted by coupled knitting-in reactions where newly arriving \γ-channel dislocations re-establish the minimum energy configuration. Here we provide microstructural evidence for knitting-out and knitting-in reactions and show that while these reactions clearly occur, dislocation network spacings stay constant. The misfit between the \γ- and the \γ\′-phase accounts for a constant network spacing. Dislocation networks are not static but represent dynamic steady state equilibrium structures in an evolving microstructure. Knitting regular networks requires climb processes which are suggested to be rate controlling. This new view of high temperature and low stress creep mechanism of SXs allows to rationalize previous results published in the literature.

}, keywords = {Creep, Dislocations, Misfit, Superalloy single crystals, Transmission electron microscopy}, issn = {1359-6454}, doi = {https://doi.org/10.1016/j.actamat.2023.119576}, url = {https://www.sciencedirect.com/science/article/pii/S1359645423009059}, author = {A.B. Parsa and D. B{\"u}rger and T.M. Pollock and G. Eggeler} } @article {1886, title = {Minor Elements and Solidification Cracking During Laser Powder-Bed Fusion of a High γ' CoNi-Base Superalloy}, journal = {Metallurgical and Materials Transactions}, volume = {54}, year = {2023}, month = {02}, pages = {1-14}, doi = {10.1007/s11661-023-06957-6}, author = {Raeker, Evan and Pusch, Kira and Forsik, St{\'e}phane and Zhou, Ning and Dicus, Austin and Ren, Qing-Qiang and Poplawsky, Jonathan and Kirka, M. and Pollock, Tresa} } @article {1881, title = {Morphological Stability of Solid-Liquid Interfaces Under Additive Manufacturing Conditions}, journal = {Acta Materialia}, volume = {250}, year = {2023}, month = {03}, pages = {118858}, doi = {10.1016/j.actamat.2023.118858}, author = {Tourret, Damien and Klemm-Toole, Jonah and Eres-Castellanos, Adriana and Rodgers, Brian and Becker, Gus and Saville, Alec and Ellyson, Ben and Johnson, Chloe and Milligan, Brian and Copley, John and Ochoa, Ruben and Polonsky, Andrew and Pusch, Kira and Haines, Michael and Fezzaa, Kamel and Sun, Tao and Clarke, Kester and Babu, Suresh and Pollock, Tresa and Clarke, Amy} } @article {1931, title = {Materials for extreme environments}, journal = {Nature Reviews Materials}, volume = {8}, year = {2022}, month = {11}, doi = {10.1038/s41578-022-00496-z}, author = {Eswarappa Prameela, Suhas and Pollock, Tresa and Raabe, Dierk and Meyers, Marc and Aitkaliyeva, Assel and Chintersingh, Kerri-Lee and Cordero, Zachary and Graham-Brady, Lori} } @article {1971, title = {Merging Machine Learning and TriBeam Tomography for 3D Defect Detection in an AM CoNi-Based Superalloy}, journal = {Microscopy and Microanalysis}, volume = {28}, year = {2022}, month = {08}, pages = {862-863}, doi = {10.1017/S1431927622003828}, author = {Lamb, James and Echlin, Mclean and Polonsky, Andrew and Geurts, Remco and Pusch, Kira and Raeker, Evan and Botman, Aurelien and Torbet, Chris and Pollock, Tresa} } @article {1996, title = {Microstructure Evolution and Tensile Properties of a Selectively Laser Melted CoNi-Base Superalloy}, journal = {Metallurgical and Materials Transactions A}, volume = {53}, year = {2022}, month = {05}, doi = {10.1007/s11661-022-06716-z}, author = {Murray, Sean and Raeker, Evan and Pusch, Kira and Frey, Carolina and Torbet, Chris and Zhou, Ning and Forsik, St{\'e}phane and Dicus, Austin and Colombo, Gian and Kirka, M. and Pollock, Tresa} } @article {1966, title = {Multi-modal Dataset of a Polycrystalline Metallic Material: 3D Microstructure and Deformation Fields}, journal = {Scientific Data}, volume = {9}, year = {2022}, month = {08}, doi = {10.1038/s41597-022-01525-w}, author = {Stinville, Jean-Charles and Hestroffer, Jonathan and Charpagne, Marie-agathe and Polonsky, Andrew and Echlin, M. and Torbet, Chris and Valle, Valery and Nygren, K. and Miller, M. and Klaas, Ottmar and Loghin, Adrian and Beyerlein, I. and Pollock, T.} } @article {2036, title = {A machine learning framework for damage mechanism identification from acoustic emissions in unidirectional SiC/SiC composites}, journal = {npj Computational Materials}, volume = {7}, year = {2021}, month = {12}, doi = {10.1038/s41524-021-00620-7}, author = {Muir, C. and Swaminathan, B. and Fields, K. and Almansour, Amjad and Sevener, Kathleen and Smith, C. and Presby, Michael and Kiser, J. and Pollock, T. and Daly, S.} } @article {2146, title = {Mechanical Metrics of Virtual Polycrystals (MechMet)}, journal = {Integrating Materials and Manufacturing Innovation}, volume = {10}, year = {2021}, month = {04}, pages = {1-21}, doi = {10.1007/s40192-021-00206-7}, author = {Dawson, Paul and Miller, Matthew and Pollock, Tresa and Wendorf, Joe and Mills, Leah and Stinville, Jean-Charles and Charpagne, Marie-agathe and Echlin, Mclean} } @article {2136, title = {Microscale Characterization of Damage Accumulation in CMCs}, journal = {Journal of the European Ceramic Society}, volume = {41}, year = {2021}, month = {05}, pages = {3082-3093}, doi = {10.1016/j.jeurceramsoc.2020.05.077}, author = {Swaminathan, B. and McCarthy, N. and Almansour, Amjad and Sevener, Kathleen and Pollock, T. and Kiser, J. and Daly, S.} } @article {2141, title = {Microstructure-Based Estimation of Strength and Ductility Distributions for α+β Titanium Alloys}, journal = {Metallurgical and Materials Transactions A}, year = {2021}, month = {04}, doi = {10.1007/s11661-021-06233-5}, author = {Echlin, Mclean and Kasemer, Matthew and Chatterjee, Kamalika and Boyce, Donald and Stinville, Jean-Charles and Callahan, Patrick and Wielewski, Euan and Park, Jun-Sang and Williams, James and Suter, Robert and Pollock, Tresa and Miller, Matthew and Dawson, Paul} } @article {2076, title = {Modeling lattice rotation fields from discrete crystallographic slip bands in superalloys}, journal = {Extreme Mechanics Letters}, volume = {49}, year = {2021}, month = {08}, pages = {101468}, doi = {10.1016/j.eml.2021.101468}, author = {Latypov, Marat and Hestroffer, Jonathan and Stinville, Jean-Charles and Mayeur, Jason and Pollock, Tresa and Beyerlein, Irene} } @article {2131, title = {Multimodal 3D Characterization of Voids in Shock-Loaded Tantalum: Implications for Ductile Spallation Mechanisms}, journal = {Acta Materialia}, volume = {215}, year = {2021}, month = {06}, pages = {117057}, doi = {10.1016/j.actamat.2021.117057}, author = {Francis, Toby and Rottmann, Paul and Polonsky, Andrew and Charpagne, Marie-agathe and Echlin, Mclean and Livescu, Veronica and Jones, David and Gray, G. and Graef, Marc and Pollock, Tresa} } @article {2051, title = {A Multi-modal Data Merging Framework for Correlative Investigation of Strain Localization in Three Dimensions}, journal = {JOM}, volume = {73}, year = {2021}, month = {09}, doi = {10.1007/s11837-021-04894-6}, author = {Charpagne, Marie-agathe and Stinville, Jean-Charles and Polonsky, Andrew and Echlin, M. and Pollock, T.} } @article {1626, title = {Measurement of elastic and rotation fields during irreversible deformation using Heaviside-digital image correlation}, journal = {Materials Characterization}, volume = {169}, year = {2020}, month = {11/2020}, pages = {110600}, abstract = {

The recent development of the high resolution and discontinuity-tolerant digital image correlation technique enables the extraction of discontinuities within a displacement field. The technique provides quantitative analysis of discontinuities arising from slip, shear bands, cracks, and grain boundary sliding in a variety of material systems, including polycrystalline metallic materials. The discontinuity-tolerant digital image correlation method can be implemented to retrieve not only quantitative discontinuity analysis but also the local strain and rotation fields that operate near these discontinuities. The present implementation includes high-resolution digital image correlation (HR-DIC) measurements collected in a scanning electron microscope for analysis of both the plastic and elastic fields that develop during deformation of polycrystalline metallic materials. The combination of the discontinuity-tolerant DIC technique with the computation of internal gradients enables extraction of non-localized strain and rotation fields during plastic deformation of a nickel-based superalloy. Therefore the lattice rotation/expansion and plastic localization that occur during deformation can be determined in a single experiment. This method is validated using synthetic images with preset deformation, and experimental measurements using the electron back scatter diffraction (EBSD) technique.

}, doi = {https://doi.org/10.1016/j.matchar.2020.110600}, url = {https://www.sciencedirect.com/science/article/abs/pii/S1044580320320714}, author = {J.C. Stinville and M.A. Charpagne and F. Bourdin and P.G. Callahan and Z. Chen and M.P. Echlin and D. Texier and J. Cormier and P. Villechaise and T.M. Pollock and V. Valle} } @article {1581, title = {Microscale characterization of damage accumulation in CMCs}, journal = {Journal of the European Ceramic Society}, year = {2020}, abstract = {

The developing roles of damage mechanisms in the failure response of SiC/SiC minicomposites was investigated by the characterization of microscale damage accumulation with respect to microstructure. A multi-modal approach combining spatially resolved acoustic emission (AE) with tensile testing in-SEM (scanning electron microscope) was used to simultaneously examine surface (observed in-SEM) and bulk damage (monitored via AE). Strong agreement was shown between the evolving crack density estimated by AE and in-SEM measurements. The following were observed: (i) in-plane matrix content and distribution impacted crack growth; (ii) spatially-distributed matrix cracks generated varying stress-dependent AE; and (iii) certain individual cracks became more probable failure locations due to unique combinations of damage mechanisms that drove their growth. This approach enabled characterizing potential failure determinants and suggests that early damage behavior is related to certain microstructural features (e.g. surface flaws), while subsequent damage behavior is coupled to interactions of local mechanisms evolving with stress.

}, keywords = {Acoustic emission, Ceramic matrix composite, Cracking, Damage initiation, Silicon carbide}, issn = {1873619X}, doi = {10.1016/j.jeurceramsoc.2020.05.077}, url = {https://doi.org/10.1016/j.jeurceramsoc.2020.05.077}, author = {Swaminathan, B. and McCarthy, N. R. and Almansour, A. S. and Sevener, K. and Pollock, T. M. and Kiser, J. D. and Daly, S.} } @conference {1591, title = {Microstructure and Tensile Properties of a CoNi-Based Superalloy Fabricated by Selective Electron Beam Melting}, booktitle = {Superalloys 2020}, year = {2020}, publisher = {Springer International Publishing}, organization = {Springer International Publishing}, abstract = {

Successful application of selective electron beam melting to a novel CoNi-based superalloy named SB-CoNi-10 is demonstrated. Crack-free as-printed microstructures exhibit excellent ductilities above 30\% and ultimate tensile strengths above 1.1 GPa at room temperature in tension. Conventional post-processing consisting of a super-solvus hot isostatic pressing (HIP), a solution heat treatment (SHT), and a low-temperature aging has been applied to remove microstructural inhomogeneities present in the as-printed microstructure. The microstructures of the as-printed and HIP+SHT+Aged alloys have been investigated to determine the effect of post-processing heat treatments on the nanoscale \γ/\γ\&$\#$39; microstructure and the mesoscale grain structure. Tensile tests have been conducted at room temperature and elevated temperatures above 850 {\textopenbullet}C to investigate mechanical properties in both the as-printed and HIP+SHT+Aged conditions. The high- temperature ductility and strength are strongly affected by the microstructure, with a mostly columnar-grained microstructure in the as-printed condition exhibiting superior ductility to the fully recrystallized microstructure in the HIP+SHT+Aged condition.

}, keywords = {Additive manufacturing, CoNi-based superalloys, Mechanical properties}, isbn = {9783030518349}, doi = {10.1007/978-3-030-51834-9}, url = {http://dx.doi.org/10.1007/978-3-030-51834-9_65}, author = {Murray, Sean P. and Pusch, Kira M. and Polonsky, Andrew T. and Torbet, Chris J. and Seward, Gareth G. E. and Nandwana, Peeyush and Kirka, Michael M. and Dehoff, Ryan R. and Zhou, Ning and Forsik, St{\'e}phane A. J. and Slye, William and Pollock, Tresa M.}, editor = {Tin, Sammy and Hardy, Mark and Clews, Justin and Cormier, Jonathan and Feng, Qiang and Marcin, John and O{\textquoteright}Brien, Chris and Suzuki, Akane} } @article {1691, title = {Multiplicity of dislocation pathways in a refractory multiprincipal element alloy}, journal = {Science}, volume = {370}, year = {2020}, pages = {95{\textendash}101}, abstract = {

Refractory multiprincipal element alloys (MPEAs) are promising materials to meet the demands of aggressive structural applications, yet require fundamentally different avenues for accommodating plastic deformation in the body-centered cubic (bcc) variants of these alloys. We show a desirable combination of homogeneous plastic deformability and strength in the bcc MPEA MoNbTi, enabled by the rugged atomic environment through which dislocations must navigate. Our observations of dislocation motion and atomistic calculations unveil the unexpected dominance of nonscrew character dislocations and numerous slip planes for dislocation glide. This behavior lends credence to theories that explain the exceptional high temperature strength of similar alloys. Our results advance a defect-aware perspective to alloy design strategies for materials capable of performance across the temperature spectrum.

}, issn = {10959203}, doi = {10.1126/science.aba3722}, author = {Wang, Fulin and Balbus, Glenn H. and Xu, Shuozhi and Su, Yanqing and Shin, Jungho and Rottmann, Paul F. and Knipling, Keith E. and Stinville, Jean Charles and Mills, Leah H. and Senkov, Oleg N. and Beyerlein, Irene J. and Pollock, Tresa M. and Gianola, Daniel S.} } @inbook {1536, title = {Multi-scale Microstructure and Property-Based Statistically Equivalent RVEs for Modeling Nickel-Based Superalloys}, booktitle = {Integrated Computational Materials Engineering (ICME): Advancing Computational and Experimental Methods}, year = {2020}, pages = {55{\textendash}90}, publisher = {Springer International Publishing}, organization = {Springer International Publishing}, address = {Cham}, abstract = {

This chapter discusses fundamental aspects of the development of statistically equivalent virtual microstructures (SEVMs) and microstructure and property-based statistically equivalent representative volume elements (M-SERVE and P-SERVE) of the Ni-based superalloy at multiple scales. The two specific scales considered for this development are the subgrain scale of intragranular \γ\thinspace\−\thinspace\γ\textasciiacutex microstructures and the polycrystalline scale of grain ensembles with annealing twins. A comprehensive suite of computational methods that can translate microstructural data in experimental methods to optimally defined representative volumes for effective micromechanical modeling is the objective of this study. The framework involves a sequence of tasks, viz., serial sectioning, image processing, feature extraction, and statistical characterization, followed by micromechanical analysis and convergence tests for statistical functions. A principal motivation behind this paper is to translate high-fidelity microstructural image data into statistics of parametric descriptors in constitutive laws governing material performance.

}, isbn = {978-3-030-40562-5}, doi = {10.1007/978-3-030-40562-5_3}, url = {https://doi.org/10.1007/978-3-030-40562-5_3}, author = {Ghosh, Somnath and Weber, George and Pinz, Maxwell and Bagri, Akbar and Pollock, Tresa M. and Lenthe, Will and Stinville, Jean-Charles and Uchic, Michael D. and Woodward, Christopher}, editor = {Ghosh, Somnath and Woodward, Christopher and Przybyla, Craig} } @article {1381, title = {A model for high temperature deformation of nanolaminate Cu-Nb composites}, journal = {Materials Science and Engineering A}, volume = {761}, year = {2019}, pages = {138016}, abstract = {

Nanolaminate composites with layer thicknesses down to 65 nm display conventional 3 stage creep behavior with creep resistance increasing as layer thickness decreases. A model for the time dependent high temperature deformation response of Cu-Nb composites is developed, and compared to creep tests performed on multilayers fabricated via accumulative roll bonding (ARB). The model assumes a continuous laminate structure of 50\% Cu and 50\% Nb in which deformation is controlled by stage II creep for the copper (\ε˙cr=A\σn) and plasticity in Nb. Regimes in which composite steady-state creep at constant stress can be achieved are identified. The modeling illustrates that strain-hardening in the niobium plays a critical role in the transient response of the multilayer, which can dominate the creep lifetime. The combination of experiments and models strongly suggest that dislocation climb mechanisms in the copper control the time-response at 400 oC for all layer thicknesses tested.

}, keywords = {Creep model, Cu-Nb, Multilayer composite, Strain hardening}, issn = {09215093}, doi = {10.1016/j.msea.2019.06.026}, url = {https://doi.org/10.1016/j.msea.2019.06.026}, author = {Avallone, Jaclyn T. and Nizolek, Thomas J. and Pollock, Tresa M. and Begley, Matthew R.} } @article {1436, title = {Measurements of plastic localization by heaviside-digital image correlation}, journal = {Acta Materialia}, volume = {157}, year = {2018}, pages = {307{\textendash}325}, abstract = {

In polycrystalline metallic materials, quantitative and statistical assessment of the plasticity in relation to the microstructure is necessary to understand the deformation processes during mechanical loading. Plastic deformation often localizes into physical slip bands at the sub-grain scale. Detrimental microstructural configurations that result in the formation and evolution of slip bands during loading require advanced strain mapping techniques for the identification of these atomically sharp discontinuities. A new discontinuity-tolerant DIC method, Heaviside-DIC, has been developed to account for discontinuities in the displacement field. Displacement fields have been measured at the scale of the physical slip bands over large areas in nickel-based superalloys by high resolution scanning electron microscopy digital image correlation (SEM DIC). However, conventional DIC methods cannot quantitatively measure plastic localization in the presence of discontinuous kinematic fields such as those produced by slip bands. The Heaviside-DIC technique can autonomously detect discontinuities, providing information about their location, inclination, and identify slip systems (in combination with orientation mapping). Using Heaviside-DIC, discontinuities are physically evaluated as sharp shear-localization events, allowing for the quantitative measure of strain amplitude nearby the discontinuities. Measurements using the new Heaviside-DIC technique are compared to conventional DIC methods for identical materials and imaging conditions.

}, keywords = {Discontinuities measurements, High resolution digital image correlation, Ren{\'e} 88DT polycrystalline superalloy, Scanning electron microscopy, Slip band offset, Slip band shearing, Slip system identification, Strain localization}, issn = {13596454}, doi = {10.1016/j.actamat.2018.07.013}, url = {https://doi.org/10.1016/j.actamat.2018.07.013}, author = {Bourdin, F. and Stinville, J. C. and Echlin, M. P. and Callahan, P. G. and Lenthe, W. C. and Torbet, C. J. and Texier, D. and Bridier, F. and Cormier, J. and Villechaise, P. and Pollock, T. M. and Valle, V.} } @article {1456, title = {Microstructure and property based statistically equivalent RVEs for intragranular γ-γ{\textquoteright} microstructures of Ni-based superalloys}, journal = {Acta Materialia}, volume = {157}, year = {2018}, pages = {245{\textendash}258}, abstract = {

This paper develops statistically equivalent RVEs or SERVEs for intragranular microstructures of Ni-based superalloys, characterized by \γ-\γ\&$\#$39; phase distribution. The SERVE represents an optimal computational domain to be used for micromechanical simulations for effective properties or response variables in the microstructure. The SERVE is further classified as a microstructure-based SERVE or M-SERVE or property-based SERVE or P-SERVE, depending on whether the statistics of morphological characteristics or convergence of chosen material properties are its determinants. Starting from FIB-SEM data for the superalloy Ren\é 88DT, the paper systematically develops a host of algorithms for generating validated statistically equivalent virtual microstructures, from which the M-SERVE is estimated from convergence of selected morphological and spatial distributions. Subsequently the P-SERVEs are established for global properties like yield strength and hardening rate, and local variables including dislocation density and the maximum resolved shear stress. Spatially-averaged quantities are found to converge quicker than the local distributions for both M-SERVE and P-SERVE.

}, keywords = {M-SERVE, Ni-based superalloys, P-SERVE, SEVM, Two-point correlation function, γ-γ{\textquoteright} distribution}, issn = {13596454}, doi = {10.1016/j.actamat.2018.07.034}, url = {https://doi.org/10.1016/j.actamat.2018.07.034}, author = {Pinz, M. and Weber, G. and Lenthe, W. C. and Uchic, M. D. and Pollock, T. M. and Ghosh, S.} } @article {1491, title = {Microstructure and Property-Based Statistically Equivalent Representative Volume Elements for Polycrystalline Ni-Based Superalloys Containing Annealing Twins}, journal = {Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science}, volume = {49}, year = {2018}, pages = {5727{\textendash}5744}, abstract = {

This paper has three major objectives related to the development of computational micromechanics models of Ni-based superalloys, containing a large number of annealing twins. The first is the development of a robust methodology for generating 3D statistically equivalent virtual polycrystalline microstructures (3D-SEVPM) of Ni-based superalloys. Starting from electron backscattered diffraction (EBSD) images of sections, the method develops distributions and correlation functions of various morphological and crystallographic parameters. To incorporate twins in the parent grain microstructure, the joint probability of the number of twins and parent grain size, and the conditional probability distributions of twin thickness and twin distance are determined. Subsequently, a method is devised for inserting twins following the distribution functions. The overall methodology is validated by successfully comparing various statistics of the virtual microstructures with 3D EBSD data. The second objective is to establish the microstructure-based statistically equivalent representative volume element or M-SERVE that corresponds to the minimum SERVE size at which the statistics of any morphological or crystallographic feature converge to that of the experimental data. The Kolmogorov\–Smirnov (KS) test is conducted to assess the convergence of the M-SERVE size. The final objective is to estimate the property-based statistically equivalent RVE or P-SERVE, defined as the smallest SERVE, which should be analyzed to predict effective material properties. The crystal plasticity finite-element model is used to simulate SERVEs, from which the overall material response is computed. Convergence plots of material properties including the yield strength and hardening rate are used to assess the P-SERVE. A smaller P-SERVE compared to the M-SERVE indicates that the characteristic features of twins implemented in determining the M-SERVE are more stringent than those for determining material properties.

}, issn = {10735623}, doi = {10.1007/s11661-018-4858-y}, url = {https://doi.org/10.1007/s11661-018-4858-y}, author = {Bagri, Akbar and Weber, George and Stinville, Jean Charles and Lenthe, William and Pollock, Tresa and Woodward, Christopher and Ghosh, Somnath} } @article {1216, title = {Materials response to glancing incidence femtosecond laser ablation}, journal = {Acta Materialia}, volume = {124}, year = {2017}, pages = {46}, chapter = {37}, doi = {https://doi.org/10.1016/j.actamat.2016.10.055}, url = {https://www.sciencedirect.com/science/article/pii/S1359645416308229}, author = {Echlin, MP and Titus, MS and Gumbsch, P and Pollock, TM} } @article {1221, title = {Measurement of Strain Localization Resulting from Monotonic and Cyclic Loading at 650 oC in Nickel Base Superalloys}, journal = {Experimental Mechanics}, volume = {57}, year = {2017}, pages = {1289{\textendash}1309}, doi = {10.1007/s11340-017-0286-y}, author = {Stinville, J. C. and Echlin, M. P. and Callahan, P. G. and Miller, V. M. and Texier, D. and Bridier, F. and Bocher, P. and Pollock, T. M.} } @article {1236, title = {Microstructural Statistics for Fatigue Crack Initiation in Polycrystalline Nickel-base Superalloys}, journal = {International Journal of Fracture}, volume = {208}, year = {2017}, pages = {240}, chapter = {221}, doi = {https://doi.org/10.1007/s10704-017-0241-z}, url = {https://link.springer.com/article/10.1007/s10704-017-0241-z}, author = {Stinville, JC and Lenthe, William C and Echlin, MP and Callahan, PG and Texier, Damien and Pollock, TM} } @article {1256, title = {Modelling the elastic properties of bi-continuous composite microstructures captured with TriBeam serial-sectioning}, journal = {Computational Materials Science}, volume = {131}, year = {2017}, pages = {187{\textendash}195}, doi = {10.1016/j.commatsci.2017.01.026}, author = {Mignone, Paul J. and Echlin, Mclean P. and Pollock, Tresa M. and Finlayson, Trevor R. and Riley, Daniel P. and Sesso, Mitchell L. and Franks, George V.} } @article {douglas2016magnetic, title = {Magnetic hardening and antiferromagnetic/ferromagnetic phase coexistence in Mn 1- x Fe x Ru 2 Sn Heusler solid solutions}, journal = {Physical Review B}, volume = {94}, number = {9}, year = {2016}, pages = {094412}, publisher = {American Physical Society}, author = {Douglas, Jason E and Levin, Emily E and Pollock, Tresa M and Castillo, Juan C and Adler, Peter and Felser, Claudia and Kr{\"a}mer, Stephan and Page, Katharine L and Seshadri, Ram} } @article {texier2016microstructural, title = {Microstructural features controlling the variability in low-cycle fatigue properties of alloy Inconel 718DA at intermediate temperature}, journal = {Metallurgical and Materials Transactions A}, volume = {47}, number = {3}, year = {2016}, pages = {1096{\textendash}1109}, publisher = {Springer US}, author = {Texier, Damien and G{\'o}mez, Ana Casanova and Pierret, St{\'e}phane and Franchet, Jean-Michel and Pollock, Tresa M and Villechaise, Patrick and Cormier, Jonathan} } @article {berman2016microstructure, title = {Microstructure and Texture Through Thixomolding and Thermomechanical Processing and the Role of Mg17Al12 Particles}, journal = {Metallurgical and Materials Transactions A}, volume = {47}, number = {6}, year = {2016}, pages = {3125{\textendash}3136}, publisher = {Springer US}, author = {Berman, Tracy D and Pollock, Tresa M and Jones, J Wayne} } @article {verma2016microstructure, title = {Microstructure Evolution of Biphasic TiNi1+ x Sn Thermoelectric Materials}, journal = {Metallurgical and Materials Transactions A}, year = {2016}, pages = {1{\textendash}12}, publisher = {Springer US}, author = {Verma, Nisha and Douglas, Jason E and Kr{\"a}mer, Stephan and Pollock, Tresa M and Seshadri, Ram and Levi, Carlos G} } @article {pebley2014microplasma, title = {Microplasma-Based Growth of Biphasic NiFe2O4/NiO Nanogranular Films for Exchange Bias Applications}, journal = {Chemistry of Materials}, volume = {26}, number = {20}, year = {2014}, pages = {6026{\textendash}6032}, publisher = {American Chemical Society}, author = {Pebley, Andrew C and Peek, Alex and Pollock, Tresa M and Gordon, Michael J} } @conference {ardeljan2014multi, title = {A multi-scale model for texture development in Zr/Nb nanolayered composites processed by accumulative roll bonding}, booktitle = {IOP Conference Series: Materials Science and Engineering}, volume = {63}, number = {1}, year = {2014}, pages = {012170}, publisher = {IOP Publishing}, organization = {IOP Publishing}, author = {Ardeljan, M and Knezevic, M and Nizolek, T and Beyerlein, IJ and Zheng, SJ and Carpenter, JS and McCabe, RJ and Mara, NA and Pollock, TM} } @article {berman2013microstructure, title = {Microstructure Characterization of Weakly Textured and Fine Grained AZ61 Sheet}, journal = {Magnesium Technology 2013}, year = {2013}, pages = {113{\textendash}118}, publisher = {Wiley Online Library}, author = {Berman, TD and Donlon, W and Hung, CK and Milligan, P and Decker, R and Pollock, TM and Jones, JW} } @article {miao2012microstructural, title = {Microstructural extremes and the transition from fatigue crack initiation to small crack growth in a polycrystalline nickel-base superalloy}, journal = {Acta Materialia}, volume = {60}, number = {6}, year = {2012}, pages = {2840{\textendash}2854}, publisher = {Pergamon}, author = {Miao, Jiashi and Pollock, Tresa M and Jones, J Wayne} } @article {berman2012microstructure, title = {Microstructure Modification and Deformation Behavior of Fine-Grained AZ61 Sheet Produced by Thixomolding and Thermomechanical Processing (TTMP)}, journal = {Magnesium Technology 2012}, year = {2012}, pages = {339{\textendash}344}, publisher = {John Wiley \& Sons, Inc.}, author = {Berman, TD and Donlon, William and Miller, VM and Decker, R and Huang, J and Pollock, TM and Jones, JW} } @article {pollock2012multifunctional, title = {Multifunctional coating interlayers for thermal-barrier systems}, journal = {MRS bulletin}, volume = {37}, number = {10}, year = {2012}, pages = {923{\textendash}931}, publisher = {Cambridge Univ Press}, author = {Pollock, TM and Lipkin, DM and Hemker, KJ} } @article {kumar2011mapping, title = {Mapping of femtosecond laser-induced collateral damage by electron backscatter diffraction}, journal = {Journal of Applied Physics}, volume = {110}, number = {8}, year = {2011}, pages = {083114}, publisher = {AIP Publishing}, author = {Kumar, Anish and Pollock, Tresa M} } @article {berman2011microstructure, title = {Microstructure Evolution in AZ61L During TTMP and Subsequent Annealing Treatments}, journal = {Magnesium Technology 2011}, year = {2011}, pages = {599{\textendash}603}, publisher = {John Wiley \& Sons, Inc.}, author = {Berman, TD and Donlon, W and Decker, R and Huang, J and Pollock, TM and Jones, JW} } @booklet {huang2010mechanical, title = {On Mechanical Properties and Microstructures of TTMP Wrought Mg Alloys}, howpublished = {Minerals, Metals and Materials Society/AIME, 420 Commonwealth Dr., P. O. Box 430 Warrendale PA 15086 USA.[np]. 14-18 Feb}, year = {2010}, publisher = {Minerals, Metals and Materials Society/AIME, 420 Commonwealth Dr., P. O. Box 430 Warrendale PA 15086 USA}, author = {Huang, Jack and Arbel, Tamir and Ligeski, Laura and McCaffrey, Jesse and Kulkarni, Sanjay and Jones, J and Pollock, Tresa and Decker, Raymond and LeBeau, Steve} } @article {madison2010modeling, title = {Modeling fluid flow in three-dimensional single crystal dendritic structures}, journal = {Acta Materialia}, volume = {58}, number = {8}, year = {2010}, pages = {2864{\textendash}2875}, publisher = {Elsevier}, author = {Madison, J and Spowart, J and Rowenhorst, D and Aagesen, LK and Thornton, K and Pollock, TM} } @article {evans2009mechanism, title = {A mechanism governing oxidation-assisted low-cycle fatigue of superalloys}, journal = {Acta Materialia}, volume = {57}, number = {10}, year = {2009}, pages = {2969{\textendash}2983}, publisher = {Elsevier}, author = {Evans, AG and He, MY and Suzuki, A and Gigliotti, M and Hazel, B and Pollock, TM} } @article {cao2009microstructural, title = {Microstructural evolution and failure characteristics of a NiCoCrAlY bond coat in {\textquotedblleft}hot spot{\textquotedblright} cyclic oxidation}, journal = {Acta Materialia}, volume = {57}, number = {13}, year = {2009}, pages = {3885{\textendash}3894}, publisher = {Elsevier}, author = {Cao, F and Tryon, B and Torbet, CJ and Pollock, TM} } @article {husseini2008mapping, title = {Mapping single-crystal dendritic microstructure and defects in nickel-base superalloys with synchrotron radiation}, journal = {Acta Materialia}, volume = {56}, number = {17}, year = {2008}, pages = {4715{\textendash}4723}, publisher = {Pergamon}, author = {Husseini, Naji S and Kumah, Divine P and Jian, Z Yi and Torbet, Christopher J and Arms, Dohn A and Dufresne, Eric M and Pollock, Tresa M and Jones, J Wayne and Clarke, Roy} } @article {mendis2006microstructural, title = {Microstructural observations of as-prepared and thermal cycled NiCoCrAlY bond coats}, journal = {Surface and Coatings Technology}, volume = {201}, number = {7}, year = {2006}, pages = {3918{\textendash}3925}, publisher = {Elsevier}, author = {Mendis, BG and Tryon, B and Pollock, TM and Hemker, KJ} } @conference {saddock2006microstructure, title = {Microstructure and mechanical properties of permanent mold cast Mg-4 A1-4 (Ca, Ce, La, or Sr) ternary alloys}, booktitle = {Symposium on Magnesium Technology 2006 (TMS 12 March 2006 to 16 March 2006)}, year = {2006}, pages = {77{\textendash}82}, publisher = {The Minerals, Metals \& Materials Society (TMS)}, organization = {The Minerals, Metals \& Materials Society (TMS)}, author = {Saddock, Nicholas and Suzuki, Akane and TerBush, Jessica and Heininger, Eric and Zindel, Jacob and Allison, John and Pollock, Tresa and Jones, J} } @article {nandy2006microstructure, title = {Microstructure and properties of blended Mg- Al alloys fabricated by semisolid processing}, journal = {Metallurgical and Materials Transactions A}, volume = {37}, number = {12}, year = {2006}, pages = {3725{\textendash}3736}, publisher = {Springer}, author = {Nandy, TK and Messing, Rebecca M and Jones, J Wayne and Pollock, Tresa M and Walukas, DM and Decker, RF} } @article {tryon2006multilayered, title = {Multilayered ruthenium-modified bond coats for thermal barrier coatings}, journal = {Metallurgical and Materials Transactions A}, volume = {37}, number = {11}, year = {2006}, pages = {3347{\textendash}3358}, publisher = {Springer}, author = {Tryon, B and Feng, Q and Pollock, TM and Wellman, RG and Nicholls, JR and Murphy, KS and Yang, J and Levi, CG} } @conference {nandy2003mechanical, title = {Mechanical Behavior of Ternary and Quaternary RuAl Alloys}, booktitle = {MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS}, volume = {753}, year = {2003}, pages = {89{\textendash}96}, publisher = {Cambridge Univ Press}, organization = {Cambridge Univ Press}, author = {Nandy, TK and Feng, Q and Banerjee, D and Gigliotti, MFX and Pollock, TM} } @article {biery2003method, title = {A method for measuring microstructural-scale strains using a scanning electron microscope: applications to $\gamma$-titanium aluminides}, journal = {Metallurgical and Materials Transactions A}, volume = {34}, number = {10}, year = {2003}, pages = {2301{\textendash}2313}, publisher = {Springer-Verlag}, author = {Biery, Nicholas and De Graef, Marc and Pollock, Tresa M} } @article {moreno2003microstructural, title = {Microstructural stability and creep of rare-earth containing magnesium alloys}, journal = {Scripta Materialia}, volume = {48}, number = {8}, year = {2003}, pages = {1029{\textendash}1034}, publisher = {Elsevier}, author = {Moreno, IP and Nandy, TK and Jones, JW and Allison, JE and Pollock, TM} } @conference {nandy2002mechanical, title = {Mechanical Behavior of Ternary and Quaternary Rual Alloys}, booktitle = {MRS Proceedings}, volume = {753}, year = {2002}, pages = {BB2{\textendash}11}, publisher = {Cambridge University Press}, organization = {Cambridge University Press}, author = {Nandy, TK and Feng, Q and Banerjee, D and Gigliotti, MFX and Pollock, TM} } @article {moreno2001microstructural, title = {Microstructural characterization of a die-cast magnesium-rare earth alloy}, journal = {Scripta Materialia}, volume = {45}, number = {12}, year = {2001}, pages = {1423{\textendash}1429}, publisher = {Elsevier}, author = {Moreno, IP and Nandy, TK and Jones, JW and Allison, JE and Pollock, TM} } @article {ott1998microstructural, title = {Microstructural development and creep deformation in equiaxed $\gamma$, $\gamma$+ $\alpha$ 2, and $\gamma$+ $\alpha$ 2+ B2 titanium aluminides}, journal = {Metallurgical and Materials Transactions A}, volume = {29}, number = {3}, year = {1998}, pages = {965{\textendash}978}, publisher = {Springer}, author = {Ott, Eric A and Pollock, Tresa M} } @conference {woodard1994microstructure, title = {Microstructure and Deformation of Ti-22Al-23Nb Orthorhombic-Based Monolithic and Composite Titanium Aluminides}, booktitle = {MRS Proceedings}, volume = {350}, year = {1994}, pages = {279}, publisher = {Cambridge University Press}, organization = {Cambridge University Press}, author = {Woodard, Shiela R and Pollock, Tresa M and others} }